Organic Structure Determination Using 2-D NMR Spectroscopy – A Problem-Based Approach is written by Jeffrey H. Simpson (Department of Chemistry Instrumentation Facility, Massachusetts Institute of Technology, Cambridge, Massachusetts) and published by Elsevier Inc. in 2008.
In Jeff Simpson words;
I wrote this book because nothing like it existed when I began to learn about the application of nuclear magnetic resonance spectroscopy to the elucidation of organic molecular structure. This book started as 40 two-dimensional (2-D) nuclear magnetic resonance (NMR) spectroscopy problem sets, but with a little cajoling from my original editor (Jeremy Hayhurst), I agreed to include problem-solving methodology in Chapters 9 and 10, and after that concession was made, the commitment to generate the first 8 chapters was a relatively small one.
Two distinct features set this book apart from other books available on the practice of NMR spectroscopy as applied to organic structure determination. The first feature is that the material is presented with a level of detail great enough to allow the development of useful ‘NMR intuition’ skills, and yet is given at a level that can be understood by a junior-level chemistry major, or a more advanced organic chemist with a limited background in mathematics and physical chemistry. The second distinguishing feature of this book is that it reflects my contention that the best vehicle for learning is to give the reader an abundance of real 2-D NMR spectroscopy problem sets. These two features should allow the reader to develop problem-solving skills essential in the practice of modern NMR spectroscopy
Beyond the lofty goal of making the reader more skilled at NMR spectra interpretation, the book has other passages that may provide utility. The inclusion of a number of practical tips for successfully conducting NMR experiments should also allow this book to serve as a useful resource.
Chapter 1: Introduction
Chapter 2: Instrumental Considerations
Chapter 3: Data Collection, Processing, and Plotting
Chapter 4: 1H and 13C Chemical Shifts
Chapter 5: Symmetry and Topicity
Chapter 6: Through-Bond Effects: Spin-Spin (J) Coupling
Chapter 7: Through-Space Effects: The Nuclear Overhauser Effect (NOE)
Chapter 8: Molecular Dynamics
Chapter 9: Strategies for Assigning Resonance to Atoms Within a Molecule
Chapter 10: Strategies for Elucidating Unknown Molecular Structures
Chapter 11: Simple Assignment Problems
Chapter 12: Complex Assignment Problems
Chapter 13: Complex Unknown Problems
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File Size: 3.19 MB, Pages: 377.
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