Free download Exploring Chemical Analysis (5th edition) written by Daniel C. Harris in pdf.
This book is intended to provide a short, interesting, elementary introduction to analytical chemistry for students of chemistry and students whose primary interests might lie outside of chemistry. I selected topics that I think should be covered in a single exposure to analytical chemistry and tried to refrain from going into more depth than necessary.
The F test for comparison of variance is introduced early in the chapter on statistics and applied to the t test for comparison of means. The meaning of statistical hypothesis testing is explained with an example from epidemiology. Two cases of standard addition with variable volume or constant volume are distinguished more clearly. Propagation of uncertainty for pH is described. A better diagram showing the working of an electronic balance and a photograph of the optical train of an ultraviolet-visible spectrophotometer are included.
The two most important ways to master this course are to work problems and to gain experience in the laboratory. Worked Examples are a principal pedagogic tool designed to teach problem solving and to illustrate how to apply what you have just read. At the end of each worked example is a similar Test Yourself question and answer.
Essential vocabulary in the text is highlighted in bold and listed in Important Terms at the end of each chapter. Other unfamiliar terms are usually italicized. The Glossary at the end of the book defines all bold terms and many italicized terms. Key Equations are highlighted and collected at the end of the chapter. Appendixes contain tables of chemical information and a discussion of balancing redox equations. The inside covers contain your trusty periodic table, physical constants, and other useful information.
Contents
- The Analytical Process
- Chemical Measurements
- Tools of the Trade
- Math Toolkit
- Statistics
- Quality Assurance and Calibration Methods
- Good Titrations
- Gravimetric and Combustion Analysis
- Introducing Acids and Bases
- Buffers
- Acid-Base Titrations
- Polyprotic Acids and Bases
- A Deeper Look at Chemical Equilibrium
- EDTA Titrations
- Electrode Potentials
- Electrode Measurements
- Redox Titrations
- Instrumental Methods in Electrochemistry
- Let There Be Light
- Spectrophotometry: Instruments and Applications
- Atomic Spectroscopy
- Principles of Chromatography and Mass Spectrometry
- Gas and Liquid Chromatography
- Chromatographic Methods and Capillary Electrophoresis
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