Free download NMR and Chemistry – An Introduction to Modern NMR Spectroscopy (4th edition) authored by J. W. Akitt and B. E. Mann in pdf.
One topic that has been finally abandoned in this edition is the old method of continuous wave NMR spectroscopy. Also, to a large extent, the old CW NMR spectra, complete with wiggle beats have been replaced by Fourier transform ones. However, we should remember that the time-shared lock systems used on the FT equipment are best understood in CW terms.
Now that multinuclear NMR spectroscopy has become routine with a wide range of nuclei being easily observable, many examples of their use have been included, ranging from sensitive nuclei such as 31P to very insensitive nuclei such as 187Os. The discussion of multipulse and two-dimensional NMR spectroscopy has also been enlarged to reflect their increasing importance. Many such experiments have become routine, with fully automated instruments running them.
Contents
- The theory of nuclear magnetization
- The magnetic field at the nucleus: nuclear screening and the chemical shift
- Internuclear spin-spin coupling
- Nuclear magnetic relaxation
- The spectrometer
- Making the spins dance
- NMR spectra of exchanging and reacting systems
- Multiple resonance and one-dimensional pulse sequences
- Two-dimensional NMR spectroscopy
- Magnetic resonance imaging and biomedical NMR
- High-resolution solid-state NMR
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