Free download Experimental Organic Chemistry: A Miniscale and Microscale Approach (6th Editionn) by John C. Gilbert & Stephen F. Martin in pdf.
The management and instruction of an introductory organic chemistry laboratory course continue to evolve, even as the core chemical principles remain unchanged. Innovation and adaptation are often driven by rising costs associated with acquiring and disposing of chemicals, as well as concerns over their potential toxicological risks to both students and the environment.
These considerations have led to the widespread adoption of scaled-down experimental techniques, commonly referred to as miniscale (or small-scale) and microscale procedures. This edition of our textbook upholds our commitment to offering both miniscale and microscale options for most experiments.
This unique approach provides instructors with maximum flexibility to tailor the course based on available equipment and glassware while addressing the specific needs of you, the student.
The miniscale approach is favored by instructors who emphasize the value of conducting experiments at a scale that enables the isolation and characterization of products using standard laboratory glassware.
Typically, the starting material quantities range from 1 to 3 grams, keeping the costs of chemical purchase and disposal manageable. This scale allows for easy handling of materials while providing students with the opportunity to refine essential techniques for product purification and characterization by comparing physical properties with those documented in scientific literature.
The microscale approach is especially attractive for minimizing the cost of purchasing and disposing of chemicals. The specialized glassware and other apparatus required for performing experiments on such small scales is now readily available.
Contents
- Introduction, Record Keeping, and Laboratory Safety
- Techniques and Apparatus
- Solids: Recrystallization and Melting Points
- Liquids: Distillation and Boiling Points
- Extraction
- Chromatography
- Stereoisomers
- Spectral Methods
- Alkanes
- Alkenes
- Alkynes
- Dienes: The Diels-Alder Reaction
- Kinetic and Thermodynamic Control of a Reaction
- Nucleophilic Aliphatic Substitution: Preparation of Alkyl Halides
- Electrophilic Aromatic Substitution
- Oxidation of Alcohols and Carbonyl Compounds
- Reduction Reactions of Double Bonds: Alkenes, Carbonyl Compounds, and lmines
- Reactions of Carbonyl Compounds
- Organometallic Chemistry
- Carboxylic Acids and Their Derivatives
- Multistep Organic Synthesis
- Polymers
- Carbohydrates
- a-Amino Acids and Peptides
- Identifying Organic Compounds
- The Literature of Organic Chemistry
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