Free download Structure Elucidation by NMR in Organic Chemistry – A Practical Guide (3rd revised edition) by Eberhard Breitmaier in pdf published by Wiley in 2002.
According to the author; “This book, based on many lectures and seminars, attempts to provide advanced undergraduates and graduate students with a systematic, readable and inexpensive introduction to the methods of structure determination by NMR. Chapter 1 starts with a deliberately concise survey of the basic terms, parameters and techniques dealt with in detail in other books, which cover the basic principles of NMR, pulse sequences as well as theoretical aspects of chemical shifts and spin-spin coupling, and which this workbook is not intended to replace. An introduction to basic strategies and tactics of structure determination using one- and two-dimensional NMR methods then follows in Chapter 2. Here, the emphasis is always on how spectra and associated parameters can be used to identify structural fragments. This chapter presents those topics that are essential for the identification of compounds or for solving structures, including atom connectivities, relative configuration and conformation, intra- and intermolecular interactions and, in some cases, molecular dynamics.Following the principle of ‘learning by doing’, Chapter 3 presents a series of case studies, providing spectroscopic details of 55 compounds that illustrate typical applications of NMR techniques in the structural characterisation of both synthetic and natural products. The level of difficulty, the sophistication of the methodology required increases from question to
Following the principle of ‘learning by doing’, Chapter 3 presents a series of case studies, providing spectroscopic details of 55 compounds that illustrate typical applications of NMR techniques in the structural characterisation of both synthetic and natural products. The level of difficulty, the sophistication of the methodology required increases from question to question so that all readers will be able to find material suited to their knowledge and ability. One can work independently, solve the problem from the spectra and check the result in the formula index, or follow the detailed solutions given in Chapter 4. The spectroscopic details are presented in a way that makes the maximum possible information available at a glance, requiring minimal page turning. Chemical shifts and coupling constants do not have to be read off from scales but are presented numerically, allowing the reader to concentrate directly on problem-solving without the need for tedious routine work.”
Contents of Structure Elucidation by NMR in Organic Chemistry
- Short Introduction to Basic Principles and Methods
- Recognition of Structural Fragments by NMR
- Problems
- Solutions to Problems
Free download Structure Elucidation by NMR in Organic Chemistry – A Practical Guide (3rd revised edition) by Eberhard Breitmaier in pdf from the following download links.
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You may also like to download Organic Structure Determination Using 2-D NMR Spectroscopy – A Problem-Based Approach by Jeffrey H. Simpson in pdf.
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