Free download Basics of Analytical Chemistry and Chemical Equilibria – A Quantitative Approach (2nd edition) authored by Brian M. Tissue in pdf.
According to the author, “This text will introduce you to analytical chemistry: the science of making quantitative measurements. Quantifying the individual components in a complex sample is an exercise in problem solving. An effective and efficient analyst will have expertise in
- sampling, sample processing, and method validation;
- the chemistry that can occur in a sample before and during analysis;
- selecting an appropriate analytical method; and
- proper record keeping, data analysis, and reporting of results
I do not attempt to be comprehensive in this text. Samples that require analysis are so diverse that it is not possible to describe every sample preparation protocol, separation method, and measurement technique. These details are contained in handbooks and method compilations, many of which are now accessible from online sources.
This text emphasizes the fundamental chemical and physical concepts that underlie the analytical methods. With an understanding of the fundamental concepts, a scientist faced with a difficult analysis can apply the most appropriate techniques, identify when a particular problem cannot be solved with existing methods, and develop new analytical methods.
The proficient analyst will also be alert to interferences and problems in analytical measurements and recognize when an “answer” might not be correct.”
Contents
Part I: Quantitative Analysis Using Reactions That Go to “completion”
- Making Measurements
- Sample Preparation, Extractions, and Chromatography
- Classical Methods
- Molecular Spectroscopy
Part II: Reactions That Do Not Go to “completion.” Equilibria in Aqueous Solutions
- Acid–base Equilibria and Activity
- Buffer Solutions and Polyprotic Acids
- Metal–ligand Complexation
- Precipitation Equilibria
Part III: Instrumental Methods and Analytical Separations
- Electroanalytical Chemistry
- Atomic Spectrometry
- Molecular Structure Determination
- Analytical Separations
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